盆地流体年代学研究新技术:方解石激光原位U-Pb定年法

刘恩涛; ZhaoJian-xin; 潘松圻; 严德天; 陆江; 郝少斌; 龚银; 邹康

doi:10.3799/dqkx.2019.958

盆地流体年代学研究新技术:方解石激光原位U-Pb定年法

doi: 10.3799/dqkx.2019.958

刘恩涛^1,2,,
ZhaoJian-xin^3,4,5,
潘松圻²,
严德天^1,3,
陆江⁶,
郝少斌¹,
龚银¹,
邹康¹

1.
中国地质大学构造与油气资源教育部重点实验室, 湖北武汉 430074
2.
中国石油勘探开发研究院, 北京 100083
3.
中国地质大学资源学院, 湖北武汉 430074
4.
Radiogenic Isotope Facility, School of Earth and Environment Sciences, The University of Queensland, Brisbane 4072
5.
中国地质科学院北京离子探针中心, 北京 100037
6.
中国海洋石油南海西部石油管理局, 广东湛江 524057

基金项目:

青岛海洋科学与技术国家实验室海洋矿产资源评价与探测技术功能实验室开放基金 KC201701

国家自然科学基金项目 41702121

中国石油科技创新基金研究项目 2018D-5007-0104

详细信息

作者简介:
刘恩涛(1986-), 男, 副教授, 主要从事沉积学、盆地分析研究

中图分类号: P597
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出版历程
- 收稿日期: 2019-01-24
- 刊出日期: 2019-03-15

A New Technology of Basin Fluid Geochronology: In-Situ U-Pb Dating of Calcite

1.
Key Laboratory of Tectonics and Petroleum Resources of Ministry of Education, China University of Geosciences, Wuhan 430074, China
2.
PetroChina Research Institute of Petroleum Exploration & Development, Beijing 100083, China
3.
Faculty of Earth Resources, China University of Geosciences, Wuhan 430074, China
4.
Radiogenic Isotope Facility, School of Earth and Environment Sciences, The University of Queensland, Brisbane 4072, Australia
5.
Beijing SHRIMP Center, Chinese Academy of Geological Sciences, Beijing 100037, China
6.
CNOOC Nanhai West Petroleum Bureau, Zhanjiang 524057, China

摘要

摘要: 流体活动是沉积盆地内最活跃的地质营力，与盆地内油气的生成、运移和成藏关系密切，精确确定流体活动历史一直是具有挑战性和前沿性的研究方向.前期对流体活动历史的研究主要依附于流体包裹体分析，该方法很难完整恢复盆地经历的所有流体事件，更无法确定流体事件活动年代.方解石是盆地流体的直接产物，对其开展年代学研究可以准确揭示盆地流体活动历史，然而目前较为成熟的同位素稀释法方解石U-Pb等时线定年成功率较低、耗时较长.近些年研发成功的方解石激光原位U-Pb定年技术可以精确确定U含量低至10×10^-9的方解石的年代，具有空间分辨率高、测试效率高的优势.该技术已成功确定多个含油气盆地流体活动历史，显示其在盆地流体研究领域具有光明的应用前景.在详细的微观鉴定和成岩观察基础上，选取不同期次的方解石样品开展方解石激光原位U-Pb定年分析，并结合C-O同位素、微量元素研究，查明盆地流体特征及其演化历史，将是未来盆地流体研究领域的重要发展方向.
- 盆地流体 /
- 方解石 /
- U-Pb定年 /
- 流体历史 /
- 激光原位ICP-MS /
- 地质年代学
Abstract: Basin fluid is the most active geological agent in sedimentary basins, having a close relationship with the generation, migration and accumulation of hydrocarbon resources.Accurate determination of fluid flow history has been a challenging and frontier research topic.In general, the previous studies of basin fluids mainly rely on the analysis of fluid inclusions, which is difficult to successfully reconstruct the events of basin fluids.More seriously, this method is unable to determine the timing of fluid flow events.Authigenic calcite is the direct product of basin fluids.Thus, accurate dating of authigenic calcite provides a new approach to determine the history of fluid flow events.In the field of calcite geochronology, the most widely used dating method was the isotope dilution U-Pb dating approach.However, this approach is time-consuming, and has a low success rate.In recent years, laser ablation technology has greatly facilitated U-Pb dating of accessory minerals (including calcite) because of its high spatial resolution and rapid data acquisition.It has been confirmed that the newly-developed in-situ U-Pb dating method is able to accurately determine the age of calcite with U content less than 10×10^-9.This method has successfully reconstructed the history of fluid flow events in the sedimentary basins, suggesting that it has a good application prospect in the field of basin fluid geochronology.In the future, it can be expected that the application of in-situ U-Pb dating of calcite together with C-O isotope and rare earth element analysis will be a significant development direction in the field of basin fluid studies.It is worth noting that the determination of stage of authigenic calcite through systematic microscopic identification and diagenetic observation is the premise of application success.
- basin fluid /
- calcite /
- U-Pb dating /
- fluid history /
- laser ablation ICP-MS /
- geochronology

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图 1 同位素稀释法方解石U-Pb测年典型实例

据Rasbury et al. (2004)

Fig. 1. The typical example of calcite ages using isotope dilution U-Pb isochrones approach

下载: 全尺寸图片幻灯片

图 2 同位素稀释法方解石U-Pb定年(a)与激光原位法(b)测试结果对比

据Robert et al.(2017)

Fig. 2. The comparison between ID-IRMS U-Pb data (a) and in-situ LA-ICPMS data (b)

下载: 全尺寸图片幻灯片

图 3 运用激光原位方解石U-Pb定年成功确定盆地断层活动带流体活动历史典型实例

数据来自Nuriel et al.(2017)

Fig. 3. The typical example showing the application of in-situ U-Pb dating method to reconstruct the history of fluid flow events in the sedimentary basin

下载: 全尺寸图片幻灯片

表 1 盆地流体年代学主要研究方法介绍

Table 1. The main methods of basin fluid flow history

研究方法	主要特点	测试仪器	代表性文献
流体包裹体法	在盆地流体研究领域中应用最为广泛, 主要用于流体期次研究, 但该方法容易受到继承性包裹体的影响, 很难准确确定流体活动时间	偏光显微镜	Worden et al. (1999)
自生伊利石定年法	主要有K-Ar、Ar-Ar及Rb-Sr等时线3种定年手段, 分选出纯净的伊利石是该方法的难点, 仅适用于碎屑岩盆地	GV Instrument 5400、Helix-MC稀有气体质谱仪及TIMS/MC-ICPMS	Uysal et al. (2001)
自生钾长石加大边定年法	通常采用激光显微探针Ar-Ar定年手段, 样品需求量小, 测试精度高, 但满足测试需求的样品较少	GV Instrument 5400和Helix-MC稀有气体质谱仪	Mark et al. (2005)
同位素稀释法方解石U-Pb测年法	在方解石年代学研究领域应用较为广泛, 但测试周期长、成功率并不高	MC-ICPMS、TIMS	Smith et al. (1991)
方解石激光原位ICP-MS U-Pb定年法	发展迅速, 测试精度高, 具有空间分辨率高、测试效率高的优势, 尚有一些技术问题需要解决	LA-HR- ICPMS、LA-MC-ICPMS	Roberts and Walker (2016); Nuriel et al. (2017)
方解石U-Th定年法	测试精度高, 但仅能测量50万年以内的样品年龄	MC-ICPMS、TIMS	Zhao et al. (2009)
方解石ESR年代学	测年的年限较长, 可从几千年到几百万年, 但主要用于断层带研究, 获得可靠的古剂量值是得到准确年龄的前提	电子顺磁(自旋)共振波谱仪	王鹏昊等(2013)

下载: 导出CSV

表 2 同位素稀释法方解石U-Pb测年代表性数据汇总

Table 2. Representative data of calcite using isotope dilution U-Pb isochrone approach

U-Pb年龄(Ma)	误差(Ma)	加权平均方差	U最大含量(10^-6)	²³⁸U/²⁰⁴Pb	样品类型	文献
0.83	0.05	0.86	0.003	18 638~226 350	洞穴方解石	Polyak et al. (2008)
2.11	0.06	2.8	0.49	20 000~120 000	方解石	Walker et al. (2006)
2.17	0.06	7.9	1.34	3 000~90 000	方解石	Walker et al. (2006)
2.19	0.47	1.6	0.001	5 849~13 744	洞穴方解石	Polyak et al. (2008)
2.24	0.08	85	1.71	6 000~50 000	方解石	Walker et al. (2006)
2.68	0.49	0.53	0.001	3 056~5 420	洞穴方解石	Polyak et al. (2008)
3.43	0.43	2.3	0.004	186~940	洞穴方解石	Polyak et al. (2008)
3.77	0.09	0.66	1.2	52 485~224 120	石笋方解石	Woodhead et al. (2006)
3.83	0.11	0.17	1.44	36 026~1 480 200	石笋方解石	Woodhead et al. (2006)
4.09	0.12	2.1	2.02	33 511~170 230	石笋方解石	Woodhead et al. (2006)
14.81	0.39	2.8	169	1 961~6 510	石灰岩方解石	Cole et al. (2005)
15.30	0.25	2.9	175	2 707~5 891	石灰岩方解石	Cole et al. (2005)
16.14	0.40	31	30.7	123.5~427.2	石灰岩方解石	Cole et al. (2005)
16.24	0.23	15	162	401~2584	石灰岩方解石	Cole et al. (2005)
80.9	11	30	0.6	22~122	方解石	Wang et al. (1998)
91.7	1.9	126	2	7.3~3 725	洞穴方解石	Lundberg et al. (2000)
211.9	2.1	2.67	2.7	114~617	方解石	Wang et al. (1998)
212.4	3.4	3.5	2.5	7.4~364	方解石	Wang et al. (1998)
271	19	877	33	637~1615	方解石	Becker (2001)
292.3	6.5	83	16.3	356~792	方解石	Becker (2001)

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表 3 激光原位方解石l > Pb定年设备LA-ICPIVIS和LA-MOICPMS格度对比数据

Table 3. he comi > arison l > etwecn in-situ LA-ICPMS and LA-MC-ICPMS U-Ph calcite data

样品名	U(10^-6)	²³⁸U/²⁰⁶Pb	²⁰⁷Pb/²⁰⁶Pb	t(Ma)	±2σ	误差率	加权平均力差	点数	数据来源	仪器类型
SFN-1	0.600	23~406	0.07~0.81	15.83	0.4	3%	1.6	26	Nuriel et al.(2017)	LV-MC-ICPMS
SFN-4	0.130	17~422	0.11~0.83	13.65	0.5	4%	1.2	16	Nuriel et al.(2017)	LV-MC-ICPMS
YG3	0.350	4.4~358	0.09~0.77	16.97	0.6	4%	2.3	48	Nuriel et al.(2017)	LV-MC-ICPMS
YF4c	1.200	1.3~266	0.33~0.82	15.53	0.5	3%	0.89	47	Nuriel et al.(2017)	LV-MC-ICPMS
AHX-1	0.140	0.50~32	0.08~0.86	209.2	0.83	< 1%	3.2	85	未发表数据	LV-MC-ICPMS
595B-2R1-84-95	0.013	0.92~8.71	0.71~0.85	115	16	14%	1.5	18	Coogan et al.(2016)	LV-HR-ICPMS
595B-3R2-12-18	0.019	2.71~20.5	0.62~0.83	86	14	16%	6.6	41	Coogan et al.(2016)	LV-HR-ILTMS
543-16R6-114.5-118	0.050	1.51~43.9	0.41~0.85	91.3	4.9	5%	1.5	42	Coogan et al.(2016)	LV-HR-ICPMS
417D-27R4-61	0.124	0.96~58.4	0.09~0.82	103.9	3.1	3%	0.31	18	Coogan et al.(2016)	LV-HR-ICPMS
418A-15R3-144	0.534	0.43~49.4	0.09~0.82	121.9	3.8	3%	4.8	28	Coogan et al.(2016)	LV-HR-ICPMS
417D-31R4-8	2.460	18.7~52.4	0.06~0.54	127.5	4.7	4%	5.3	53	Coogan et al.(2016)	LV-HR-ILTMS
TJN-6-1	0.108	121~162	0.12~0.28	37.7	1.9	5%	2.4	35	Roberts and Walker (2016)	LV-HR-ICPMS
MOL-1-2	0.037	22.2~144	0.05~0.40	40.1	4.8	12%	5.3	29	Roberts and Walker (2016)	LV-HR-ICPMS

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