豫南新县岩体地球化学、年代学和Hf同位素特征及地质意义

刘清泉; 邵拥军; 陈昕梦; 刘忠法; 张喆

doi:10.3799/dqkx.2016.507

豫南新县岩体地球化学、年代学和Hf同位素特征及地质意义

doi: 10.3799/dqkx.2016.507

刘清泉^1,2,3,,
邵拥军^1,2, ,,
陈昕梦⁴,
刘忠法^1,2,
张喆³

1.
中南大学有色金属成矿预测与地质环境监测教育部重点实验室，湖南长沙 410083
2.
中南大学地球科学与信息物理学院，湖南长沙 410083
3.
河南省有色金属地质勘查总院，河南郑州 450052
4.
河南省有色金属地质矿产局第七地质大队，河南郑州 450016

基金项目:

中国地质调查局地质矿产调查评价专项 12120113091200

中南大学创新驱动计划项目 2015CX008

详细信息

作者简介:
刘清泉(1982-)，男，博士研究生，矿产普查与勘探专业.E-mail: liu_qingquan@126.com

通讯作者:
邵拥军，E-mail: shaoyongjun@126.com

中图分类号: P618
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出版历程
- 收稿日期: 2015-03-28
- 刊出日期: 2016-08-15

Petrogeochemistry, Geochronology and Hf Isotopes of the Monzogranite from Xinxian, Southern Region in Henan Province

Liu Qingquan^{1,2,3
,},
Shao Yongjun^{1,2
, ,},
Chen Xinmeng⁴,
Liu Zhongfa^1,2,
Zhang Zhe³

1.
Key Laboratory of Metallogenic Prediction of Nonferrous Metals and Geological Environment Monitoring, Ministry of Education, Central South University, Changsha 410083, China
2.
School of Geosciences and Info-Physics, Central South University, Changsha 410083, China
3.
Henan Nonferrous Metals Geological Exploration Institute, Zhengzhou 450052, China
4.
The Seventh Geological Brigade of Henan Nonferrous Metals Geological Mineral Resources Bureau, Zhengzhou 450016, China

摘要

摘要: 新县岩体位于秦岭-大别造山带上，对其进行系统的岩石地球化学探讨有助于加深对秦岭-大别造山带中生代构造-岩浆演化及地球动力学背景的认识.岩石地球化学分析结果显示，SiO₂含量为74.94%~78.16%，K₂O含量为3.87%~5.86%，Na₂O含量为3.82%~4.24%，Al₂O₃含量为12.38%~13.57%，具有高钾钙碱性和过铝质(A/CNK=1.05~1.11) 特征.岩石稀土总量较低(42.67×10^-6~110.45×10^-6)，轻稀土元素相对富集，重稀土元素相对亏损，具有Eu的负异常，岩体富集Rb、U、Hf和Y，亏损Ba、Nb、Ta和Ti，显示出Ⅰ型高分异花岗岩的特点.3个期次岩石的U-Pb年龄分别为153.4±1.1 Ma、146.4±1.6 Ma和131.6±1.8 Ma.锆石Hf同位素分析结果表明，新县岩体的ε_Hf(t)值为-24.5~-20.3，位于地幔演化线之下，t_DM2值为2.68~2.93 Ga，指示其源于扬子板块北缘的古老地壳，其组成类似于扬子板块北缘TTG型岩浆岩.结合区域地质背景，新县岩体形成于扬子陆块与华北陆块碰撞造山后的陆内伸展环境，对应的地球动力学背景为晚侏罗世-早白垩世地壳从挤压收缩向区域性伸展的构造体制大转换过程和大规模的地壳伸展和岩石圈减薄时期.
- 大别山 /
- 新县 /
- 花岗岩 /
- 岩石学 /
- 地球化学 /
- 年代学 /
- Hf同位素
Abstract: Xinxian monzogranites are located at the Qinling-Dabie orogenic belt, and a systematic geochemical study can facilitate further studies on the Mesozoic tectono-magmatic evolution and the geodynamics background of Qinling-Dabie orogenic belt. This paper presents geochemistry, zircon U-Pb geochronology, and Hf-isotopic data of the rocks, with the aim of constraining their petrogenesis, sources and tectonic implications. The geochemical analysis shows that Xinxian monzogranites are characterized by SiO₂=74.94%-78.16%, K₂O=3.87%-5.86%, Na₂O=3.82%-4.24%, Al₂O₃=12.38%-13.57%, A/CNK=1.05-1.11; the rocks are enriched in LREE, depleted HREE and negative Eu anomalies, enriched in Rb, U, Hf, Y and depleted Ba, Nb, Ta, Ti, which indicates that Xinxian monzogranites are peraluminous, high-K calc-alkaline Ⅰ-type granite. The three stages yield LA-ICP-MS zircon U-Pb ages 153.4±1.1 Ma, 146.4±1.6 Ma and 131.6±1.8 Ma respectively. According to zircon Hf isotope analysis, the ε_Hf(t) values of the granite range from -24.5 to -20.3, which locates below the depleted mantle line. The t_DM2 values range from 2.68 to 2.93 Ga, which indicates the monzogranites resulted from the lower crust of Yangtze Block. The component of the monzogranite is similar to that of Neoproterozoic TTG magmatic rocks. Xinxian monzogranites were emplaced after the major collisional period of the North China block and Yangtze block, in the post-collisional tectonic setting under the regional extension mechanism. The geodynamics setting is the transformation of tectonic regime of the Late Jurassic-Early Cretaceous and large-scale lithosphere delaminating thinning under post stretching mechanism.
- Dabie mountain /
- Xinxian /
- monzogranite /
- petrology /
- geochemistry /
- geochronology /
- Hf isotope

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图 1 新县花岗岩体地质简图

1.第四系；2.白垩系下统陈棚组；3.泥盆系南湾组；4.震旦系-奥陶系肖家庙组；5.中元古界浒湾组上段；6.中元古界浒湾组下段；7.下元古界七角山组；8.下元古界新县组；9.下元古界卡房组；10.辉长岩；11.震旦系花岗岩；12.燕山期石英二长岩；13.燕山期花岗斑岩；14.燕山期二长花岗岩；15.断层；16.地质界线；17.花岗斑岩脉；18.采样位置；据陈伟等(2013)修改

Fig. 1. Geological sketch of the Xinxian granitic batholith in Henan Province

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图 2 二长花岗岩岩相学特征

a.中粗粒二长花岗岩；b.中粒二长花岗岩；c.细粒二长花岗岩；d.中粗粒二长花岗岩结构；e.中粒二长花岗岩结构；f.细粒二长花岗岩结构.Qtz.石英；Bt.黑云母；Pth.条纹长石；Pl.斜长石；Kfs.钾长石

Fig. 2. Petrography of the monzogranite

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图 3 新县二长花岗岩中锆石代表性阴极发光照片(a)；中粗粒二长花岗岩(X-01) 锆石U-Pb谐和图(b)；中粒二长花岗岩(X-03) 锆石U-Pb谐和图(c)和细粒二长花岗岩(X-05) 锆石U-Pb谐和图(d)

Fig. 3. CL images of representative zircons in the Xinxian monzogranite with analytical positions (a), the zircon U-Pb concordian of the medium-coarse monzogranite (X-01) (b), the zircon U-Pb concordian of the medium monzogranite (X-03) (c) and the zircon U-Pb concordian of the fine monzogranite (X-05) (d)

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图 4 新县二长花岗岩K₂O-SiO₂(a)和ANK-ACNK(b)关系

图a据Rickwood(1989)

Fig. 4. K₂O-SiO₂ (a) and ANK-ACNK (b) relations of the Xinxian monzogranite

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图 5 新县二长花岗岩Harker图解

Fig. 5. Harker diagram of the Xinxian monzogranite

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图 6 新县二长花岗岩原始地幔标准化微量元素蛛网图(a)与球粒陨石标准化稀土元素分布模式(b)

Fig. 6. PM-normalised trace element spider diagram (a) and chondrite-normalised REE pattern (b) of the Xinxian monzogranite

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图 7 新县二长花岗岩Q-A-P图解

Q.石英；A.碱性长石；P.斜长石；据Bowden and Kinnaird(1984)

Fig. 7. Q-A-P diagram of the Xinxian monzogranite

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图 8 (Na₂O+K₂O)/CaO-Zr+Nb+Ce+Y和(Al₂O₃+CaO)/(Na₂O+K₂O+TFeO)-100×(TFeO+MgO+TiO₂)/SiO₂关系

图a据Whalen et al.(1987)，图b据Sylvester(1989)

Fig. 8. (Na₂O+K₂O)/CaO-Zr+Nb+Ce+Y and (Al₂O₃+CaO)/(Na₂O+K₂O+TFeO)-100×(TFeO+MgO+TiO₂)/SiO₂ relations

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图 9 新县二长花岗岩REE分布模式(a)及Sr-Yb关系(b)

据张旗等(2006)

Fig. 9. REE pattern (a) and Sr-Yb relation (b) for the Xinxian monzogranite

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图 10 新县二长花岗岩造岩矿物结晶分异判别关系

PlAn50.斜长石(An=50)；PlAn15.斜长石(An=15)；Kfs.钾长石；Bt.黑云母；Ms.白云母；Grt.石榴子石；Amp.角闪石；据Janoušek et al.(2004)

Fig. 10. Ba-Sr and Rb-Sr relations for the Xinxian monzogranite

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图 11 新县二长花岗岩锆石ε_Hf(t)-t关系

Fig. 11. Relation of Zircon ε_Hf(t) and t for the Xinxian monzogranite

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图 12 新县二长花岗岩构造环境判别关系

a.Al₂O₃-SiO₂；b.TFeO/(TFeO+MgO)-SiO₂；c.R₁-R₂；d.Rb-Y+Nb；图a, b据Pearce(1996)；图c, d据Batchelor and Bowden(1985)；POG.后造山花岗岩；IAG.岛弧花岗岩；CAG.大陆弧花岗岩；CCG.大陆碰撞花岗岩；RRG.裂谷型花岗岩；CEUG.大陆造陆隆升花岗岩

Fig. 12. Discriminant relations of tectonic environment of the Xinxian monzogranite

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图 13 新县二长花岗岩构造环境的lg(CaO/(K₂O+Na₂O))-SiO₂判别关系

据Brown(1982)修改

Fig. 13. The lg(CaO/(K₂O+Na₂O))-SiO₂ discriminant relation of tectonic environment of the Xinxian monzogranite

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表 1 新县二长花岗岩LA-ICP-MS锆石U-Pb分析结果

Table 1. LA-ICP-MS zircon U-Pb data for the Xinxian monzogranite

测试点号	Th (10^-6)	U (10^-6)	Th/U	²⁰⁷Pb/²⁰⁶Pb	1σ	²⁰⁷Pb/²³⁵U	1σ	²⁰⁶Pb/²³⁸U	1σ	²⁰⁸Pb/²³²Th	1σ	年龄(Ma)
测试点号	Th (10^-6)	U (10^-6)	Th/U	²⁰⁷Pb/²⁰⁶Pb	1σ	²⁰⁷Pb/²³⁵U	1σ	²⁰⁶Pb/²³⁸U	1σ	²⁰⁸Pb/²³²Th	1σ	²⁰⁷Pb/²³⁵U	1σ	²⁰⁶Pb/²³⁸U	1σ	²⁰⁸Pb/²³²U	1σ
X-01-01	2 542	2 136	1.19	0.055 1	0.001 0	0.155 5	0.003 1	0.020 4	0.000 3	0.006 0	0.000 1	147	3	130	2	121	3
X-01-02	3 205	2 343	1.37	0.047 1	0.000 9	0.135 9	0.002 8	0.020 8	0.000 2	0.006 3	0.000 1	129	3	132	2	126	3
X-01-03	2 839	2 259	1.26	0.052 1	0.001 1	0.148 6	0.003 4	0.020 5	0.000 2	0.006 3	0.000 2	141	3	131	2	127	3
X-01-06	182	152	1.20	0.051 4	0.003 5	0.146 3	0.008 8	0.021 6	0.000 5	0.006 4	0.000 2	139	8	138	3	128	5
X-01-07	3 170	2 295	1.38	0.050 9	0.001 0	0.141 1	0.002 7	0.020 0	0.000 2	0.006 3	0.000 1	134	2	128	1	126	3
X-01-08	357	292	1.22	0.057 2	0.003 7	0.174 0	0.013 0	0.021 3	0.000 4	0.007 5	0.000 3	163	11	136	2	152	7
X-01-09	3 580	2 777	1.29	0.049 4	0.001 0	0.139 2	0.002 9	0.020 3	0.000 2	0.006 4	0.000 2	132	3	130	2	129	3
X-01-10	4 873	2 774	1.76	0.050 3	0.001 2	0.145 5	0.003 7	0.020 9	0.000 3	0.006 9	0.000 2	138	3	133	2	139	4
X-01-11	2 791	2 250	1.24	0.048 9	0.001 1	0.139 1	0.003 5	0.020 5	0.000 3	0.006 8	0.000 2	132	3	131	2	137	4
X-01-12	5 125	2 790	1.84	0.047 9	0.000 9	0.134 5	0.002 8	0.020 3	0.000 2	0.006 7	0.000 1	128	2	129	1	134	3
X-01-14	2 406	2 374	1.01	0.054 0	0.001 2	0.160 5	0.004 5	0.021 3	0.000 3	0.006 8	0.000 2	151	4	136	2	136	3
X-03-01	3 590	5 224	0.69	0.057 0	0.001 1	0.180 2	0.003 4	0.022 7	0.000 2	0.006 9	0.000 2	168	3	144	1	140	3
X-03-02	3 724	6 079	0.61	0.051 0	0.000 9	0.159 4	0.003 1	0.022 4	0.000 2	0.006 7	0.000 2	150	3	143	1	134	3
X-03-03	2 650	3 437	0.77	0.054 1	0.001 1	0.172 5	0.004 8	0.022 8	0.000 4	0.007 3	0.000 2	162	4	145	3	147	4
X-03-04	2 694	4 649	0.58	0.079 6	0.002 2	0.235 5	0.006 8	0.021 2	0.000 2	0.008 3	0.000 3	215	6	135	2	166	7
X-03-06	655	1 064	0.62	0.053 1	0.002 0	0.168 3	0.005 7	0.023 1	0.000 3	0.007 6	0.000 2	158	5	147	2	153	4
X-03-07	2 914	4 189	0.70	0.056 8	0.001 4	0.180 5	0.004 5	0.022 9	0.000 3	0.006 9	0.000 2	168	4	146	2	139	4
X-03-08	4 121	5 773	0.71	0.054 3	0.001 0	0.171 7	0.004 0	0.022 7	0.000 3	0.007 2	0.000 2	161	4	144	2	145	4
X-03-10	4 225	4 888	0.86	0.081 2	0.002 1	0.239 2	0.007 0	0.021 1	0.000 3	0.008 2	0.000 2	218	6	134	2	165	4
X-03-12	4 157	5 321	0.78	0.061 4	0.002 2	0.179 8	0.005 7	0.021 4	0.000 3	0.007 6	0.000 2	168	5	137	2	153	4
X-03-13	5 917	6 992	0.85	0.047 8	0.000 8	0.154 0	0.003 0	0.023 2	0.000 3	0.007 1	0.000 2	145	3	148	2	144	4
X-03-14	4 375	4 597	0.95	0.060 0	0.001 2	0.187 4	0.004 5	0.022 5	0.000 3	0.007 4	0.000 2	174	4	143	2	148	3
X-03-15	2 048	4 056	0.50	0.053 9	0.001 2	0.165 3	0.004 3	0.022 0	0.000 3	0.007 9	0.000 2	155	4	140	2	159	5
X-05-01	4 557	14 296	0.32	0.051 4	0.000 8	0.173 1	0.002 9	0.024 1	0.000 2	0.006 8	0.000 3	162	3	153	1	138	6
X-05-02	3 687	4 629	0.80	0.090 4	0.002 0	0.303 4	0.008 3	0.023 9	0.000 3	0.009 4	0.000 5	269	6	152	2	189	9
X-05-03	1 922	3 688	0.52	0.083 4	0.003 3	0.278 7	0.003 1	0.024 3	0.001 0	0.011 7	0.000 8	250	10	155	6	235	17
X-05-04	9 506	17 079	0.56	0.053 3	0.001 0	0.178 6	0.004 1	0.023 9	0.000 2	0.007 2	0.000 3	167	4	152	1	145	6
X-05-05	7 929	22 043	0.36	0.068 1	0.003 0	0.238 3	0.004 4	0.024 2	0.000 3	0.010 1	0.000 6	217	12	154	2	203	12
X-05-07	3 471	13 938	0.25	0.053 6	0.001 0	0.176 5	0.003 1	0.023 8	0.000 3	0.007 5	0.000 2	165	3	152	2	152	4
X-05-08	2 275	6 130	0.37	0.0902	0.001 6	0.305 1	0.006 4	0.024 4	0.000 3	0.013 3	0.000 4	270	5	155	2	267	7
X-05-09	6 837	20 129	0.34	0.054 5	0.000 7	0.183 2	0.003 0	0.024 2	0.000 3	0.010 5	0.000 2	171	3	154	2	211	5
X-05-10	6 592	21 885	0.30	0.091 1	0.003 0	0.307 5	0.001 6	0.024 3	0.000 4	0.017 5	0.000 9	272	9	155	2	350	19
X-05-11	7 229	19 846	0.36	0.048 4	0.000 8	0.160 8	0.003 6	0.023 9	0.000 3	0.007 9	0.000 2	151	3	152	2	159	5
X-05-12	7 081	24 836	0.29	0.059 0	0.001 8	0.197 7	0.006 8	0.024 0	0.000 3	0.010 7	0.000 5	183	6	153	2	215	11
X-05-13	5 247	15 865	0.33	0.052 8	0.001 1	0.178 3	0.003 7	0.024 4	0.000 3	0.007 8	0.000 2	167	3	155	2	156	4
X-05-14	13 518	31 847	0.42	0.045 9	0.001 1	0.152 3	0.003 6	0.023 9	0.000 2	0.006 7	0.000 2	144	3	152	2	134	5

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表 2 新县二长花岗岩主量元素(%)、微量和稀土元素(10^-6)分析结果

Table 2. Major elements (%), trace elements and rare earth elements (10^-6) composition of Xinxian monzogranite

样品号	X-01	X-02	X-03	X-04	X-05	X-06
SiO₂	78.16	77.32	75.75	75.24	75.62	74.94
Al₂O₃	12.38	12.38	13.57	13.54	13.33	13.52
Fe₂O₃	0.62	0.66	0.78	0.95	1.09	1.06
MgO	0.06	0.05	0.09	0.10	0.08	0.11
CaO	0.27	0.24	0.50	0.58	0.36	0.39
Na₂O	3.82	3.94	4.24	4.24	3.83	4.07
K₂O	4.16	3.87	4.50	4.45	4.86	4.65
MnO	0.01	0.01	0.04	0.06	0.02	0.02
TiO₂	0.04	0.03	0.08	0.05	0.09	0.10
P₂O₅	0.006	0.006	0.011	0.010	0.008	0.009
LOI	0.45	0.54	0.35	0.27	0.55	0.65
Total	99.98	99.05	99.91	99.49	99.84	99.52
TFeO	0.62	0.66	0.78	0.95	1.09	1.06
A/CNK	1.10	1.11	1.06	1.05	1.09	1.09
A/NK	1.15	1.16	1.15	1.15	1.15	1.15
Mg^#	16.09	13.05	18.60	17.25	12.69	17.05
R₁	2 874	2 872	2 478	2 460	2 530	2 459
R₂	276	275	326	335	306	316
Q	39.43	39.46	32.68	32.20	33.92	32.68
An	1.31	1.17	2.42	2.84	1.75	1.90
Ab	32.49	33.86	36.05	36.18	32.66	34.85
Or	24.71	23.23	26.72	26.52	28.94	27.81
Rb	393.0	365.0	311.0	307.0	216.0	196.5
Ba	40	30	120	130	260	250
Th	20	20	30	20	20	20
U	10	10	10	10	10	10
Nb	41.3	37.5	33.3	25.8	22.6	23.1
Ta	4.8	4.3	2.8	2.1	1.8	1.9
Pb	42	40	39	39	25	29
Sr	11	11	42	44	49	49
Zr	112	134	141	120	140	127
Hf	5.9	8.0	6.2	4.7	5.0	4.8
Ti	240	180	480	300	540	600
Y	13.4	16.0	10.1	8.8	12.8	11.7
Nb/Ta	8.60	8.72	11.89	12.29	12.56	12.16
Zr/Hf	18.98	16.75	22.74	25.53	28.00	26.46
La	8.9	12.1	21.6	15.4	24.8	28.5
Ce	18.9	26.1	38.2	26.7	44.4	51.0
Pr	2.05	2.77	3.53	2.51	4.67	5.13
Nd	6.1	8.9	10.5	7.4	14.6	15.7
Sm	1.23	1.75	1.58	1.08	2.24	2.84
Eu	0.05	0.07	0.17	0.15	0.31	0.32
Gd	0.95	1.23	0.93	0.76	1.67	1.80
Tb	0.16	0.21	0.17	0.12	0.28	0.26
Dy	1.21	1.45	0.97	0.85	1.76	1.77
Ho	0.25	0.33	0.22	0.18	0.36	0.36
Er	0.93	1.11	0.88	0.62	1.22	0.96
Tm	0.18	0.20	0.13	0.11	0.20	0.17
Yb	1.54	1.81	1.17	0.90	1.35	1.48
Lu	0.22	0.27	0.18	0.12	0.18	0.16
∑REE	42.67	58.30	80.23	56.90	98.04	110.45
LREE/HREE	6.84	7.82	16.25	14.55	12.97	14.87
(La/Yb)_N	4.15	4.80	13.24	12.27	13.18	13.81
δEu=Eu/Eu^*	0.14	0.14	0.39	0.48	0.47	0.40
T_Zr	807	824	825	809	826	816
注：主量元素单位为%，微量元素单位为10^-6；LOI为烧失量，单位为%；T_Zr单位为℃；δEu=Eu/Eu^*=2Eu_N/(Sm_N+Gd_N)，其中N为球粒陨石标准化值(引自Sun and Mcdonough, 1989)；TFeO=FeO+0.899 8×Fe₂O₃；A/CNK=摩尔Al₂O₃/(CaO+Na₂O+K₂O)；A/NK=摩尔Al₂O₃/(Na₂O+K₂O)；Mg^#=100×摩尔Mg(Mg+TFe²⁺)；里特曼指数σ=(Na₂O+K₂O)²/(SiO₂-43)；AR=[Al₂O₃+CaO+(Na₂O+K₂O)]/[Al₂O₃+CaO-(Na₂O+K₂O)]；R₁=摩尔[4Si-11(Na+K)-2(Fe+Ti)]；R₂=摩尔(6Ca+2Mg+Al)；T_Zr=12 900/[2.95+0.85M+ln(496 000/Zr_melt)]-273.15，M=(Na+K+2Ca)/(Al×Si)，Zr_melt为锆含量(Watson and Harrison, 1983).

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表 3 新县二长花岗岩的锆石Hf同位素组成

Table 3. Zircon Hf isotope compositions of Xinxian monzogranite

测试点号	t(Ma)	¹⁷⁶Yb/¹⁷⁷Hf	¹⁷⁶Lu/¹⁷⁷Hf	¹⁷⁶Hf/¹⁷⁷Hf	2σ	ε_Hf(t)	t_DM1(Ma)	t_DM2(Ma)
X-01-01	130	0.089 913	0.002 230	0.282 019	0.000 014	-24.0	1 793	2 790
X-01-02	132	0.050 669	0.001 201	0.282 002	0.000 019	-24.5	1 768	2 876
X-01-03	131	0.069 408	0.001 663	0.282 044	0.000 016	-23.0	1 731	2 915
X-01-06	138	0.157 415	0.003 910	0.282 022	0.000 018	-23.9	1 874	2 824
X-01-07	128	0.071 049	0.001 659	0.282 089	0.000 018	-21.5	1 666	2 877
X-01-08	136	0.057 694	0.001 426	0.282 082	0.000 016	-21.6	1 666	2 722
X-01-09	130	0.121 267	0.003 078	0.282 026	0.000 016	-23.8	1 825	2 745
X-01-10	133	0.121 524	0.003 062	0.282 062	0.000 015	-22.5	1 771	2 861
X-01-11	131	0.105 876	0.002 557	0.282 077	0.000 014	-21.9	1 725	2 785
X-01-12	129	0.045 616	0.001 050	0.282 049	0.000 016	-22.8	1 695	2 751
X-01-14	136	0.124 686	0.003 099	0.282 017	0.000 015	-24.0	1 839	2 810
X-03-01	144	0.117 658	0.004 171	0.282 017	0.000 020	-23.9	1 895	2 886
X-03-02	143	0.068 153	0.002 372	0.282 067	0.000 014	-22.0	1 731	2 894
X-03-03	145	0.074 545	0.002 578	0.282 037	0.000 016	-23.1	1 783	2 786
X-03-04	135	0.086 447	0.002 916	0.282 067	0.000 016	-22.2	1 757	2 851
X-03-06	147	0.049 355	0.001 761	0.282 055	0.000 020	-22.3	1 719	2 777
X-03-07	146	0.080 706	0.002 782	0.282 004	0.000 016	-24.2	1 842	2 814
X-03-08	144	0.084 147	0.002 919	0.282 050	0.000 016	-22.7	1 781	2 925
X-03-10	134	0.097 889	0.003 540	0.282 040	0.000 021	-23.3	1 828	2 822
X-03-12	137	0.077 212	0.002 664	0.282 036	0.000 019	-23.3	1 790	2 835
X-03-13	148	0.097 509	0.003 229	0.282 090	0.000 019	-21.2	1 737	2 847
X-03-14	143	0.055 312	0.001 808	0.282 061	0.000 015	-22.2	1 713	2 738
X-03-15	140	0.065 349	0.002 206	0.282 027	0.000 016	-23.5	1 780	2 798
X-05-01	153	0.137 905	0.004 453	0.282 093	0.000 015	-21.1	1 795	2 869
X-05-02	152	0.024 449	0.000 956	0.282 063	0.000 006	-21.8	1 671	2 737
X-05-03	155	0.084 474	0.002 964	0.282 059	0.000 016	-22.1	1 770	2 802
X-05-04	152	0.077 676	0.002 707	0.282 070	0.000 019	-21.8	1 742	2 813
X-05-05	154	0.051 021	0.001 713	0.282 071	0.000 016	-20.3	1 839	2 787
X-05-07	152	0.077 947	0.002 638	0.282 067	0.000 038	-21.9	1 744	2 682
X-05-08	155	0.173 258	0.005 759	0.282 062	0.000 019	-22.3	1 914	2 795
X-05-09	154	0.144 987	0.004 498	0.282 045	0.000 014	-22.8	1 870	2 807
X-05-10	155	0.166 763	0.005 287	0.282 073	0.000 017	-21.9	1 871	2 843
X-05-11	152	0.152 313	0.004 866	0.282 109	0.000 016	-20.6	1 792	2 784
X-05-12	153	0.015 606	0.000 507	0.282 066	0.000 019	-21.7	1 648	2 702
X-05-13	155	0.134 066	0.004 520	0.282 062	0.000 016	-22.2	1 847	2 797
X-05-14	152	0.137 464	0.004 262	0.282 063	0.000 016	-22.2	1 831	2 808
注：ε_Hf(t)=10 000×{[(¹⁷⁶Hf/¹⁷⁷Hf)_s-(¹⁷⁶Lu/¹⁷⁷Hf)_s×(e^λt-1)]/[(¹⁷⁶Hf/¹⁷⁷Hf)_CHUR.0-(¹⁷⁶Lu/¹⁷⁷Hf)_CHUR×(e^λt-1)]-1}; t_DM1=1/λ×ln{1+[(¹⁷⁶Hf/¹⁷⁷Hf)_s-(¹⁷⁶Hf/¹⁷⁷Hf)_DM]/[(¹⁷⁶Lu/¹⁷⁷Hf)_s-(¹⁷⁶Lu/¹⁷⁷Hf)_DM]}; t_DM2=1/λ×ln{1+[(¹⁷⁶Hf/¹⁷⁷Hf)_s.t-(¹⁷⁶Hf/¹⁷⁷Hf)_DM.t]/[(¹⁷⁶Lu/¹⁷⁷Hf)_c-(¹⁷⁶Lu/¹⁷⁷Hf)_DM]}+t; (¹⁷⁶Hf/¹⁷⁷Hf)_s和(¹⁷⁶Lu/¹⁷⁷Hf)_s为样品测定值; (¹⁷⁶Hf/¹⁷⁷Hf)_CHUR.0=0.282 772, (¹⁷⁶Lu/¹⁷⁷Hf)_CHUR=0.033 2, (¹⁷⁶Hf/¹⁷⁷Hf)_DM=0.283 25, (¹⁷⁶Lu/¹⁷⁷Hf)_DM=0.038 4(Rubatto and Gebauer, 2000); λ=1.867×10^-11/a (Griffin et al., 2000); (¹⁷⁶Lu/¹⁷⁷Hf)_c=0.015; t为锆石结晶时间，单位为Ma.

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